Buchi Rotavapo R-215 Manual de usuario

093076 enR�210/215Rotavapor®Operation Manual

2 Safety10 R-210/215 Operation Manual, Version FOptional• P+G is a unique protective layer for glass components. It offers improved mechanical damag

3 Technical data11 R-210/215 Operation Manual, Version F3 Technical dataThis chapter introduces the reader to the instrument specifications. It conta

3 Technical data12 R-210/215 Operation Manual, Version FOrder number:2 31x x x x x xRotavapor R-215The vapor temperature sensor is comprised in the s

3 Technical data13 R-210/215 Operation Manual, Version FOrder number:2 3 x x1x x x xVapor duct SJ 29/32Order number:2 3x x2x x x xVapor duct SJ 24/40

3 Technical data14 R-210/215 Operation Manual, Version FOrder number:2 3x x xCx x xGlass assembly C• Dry ice condenser• For distillation of solven

3 Technical data15 R-210/215 Operation Manual, Version FOrder number:2 3x x xEx x xGlass assembly E• Descending condenser with expansion vessel• I

3 Technical data16 R-210/215 Operation Manual, Version FOrder number:2 3x x xYx x xGlass assembly BY• Vertical condenser with additional double jac

3 Technical data17 R-210/215 Operation Manual, Version FOrder number:2 3x x x x x1xVacuum Controller V-850, 100–230 V 50/60 HzOrder number:2 3x x x x

3 Technical data18 R-210/215 Operation Manual, Version FOrder number:2 3x x x x x x2Valve unitTable 3-1: Standard accessoriesProduct Order numberCool

3 Technical data19 R-210/215 Operation Manual, Version F3.1.3 Optional accessoriesTable 3-2: Optional accessoriesProduct Order numberVacuum Pump V-7

3 Technical data20 R-210/215 Operation Manual, Version FTable 3-2: Optional accessories (cont.)Product Order numberF-1XX 230 VF-100 Model 500 Watt fix

3 Technical data21 R-210/215 Operation Manual, Version FTable 3-2: Optional accessories (cont.)Product Order numberHeating bath B-491 with digital di

3 Technical data22 R-210/215 Operation Manual, Version F3.1.4 UpgradeTable 3-3: Upgrade R-210 to R-215 - optionalProduct Order numberUpgrade R-210 t

3 Technical data23 R-210/215 Operation Manual, Version F3.3 Technical data overviewTable 3-5: Technical dataR-210 Rotavapor without displayR-215 Rot

3 Technical data24 R-210/215 Operation Manual, Version F3.4 Solvent tableTable 3-6: Solvent tableSolvent Formula Molar mass in g/molEvaporation ener

4 Description of function25 R-210/215 Operation Manual, Version F4 Description of functionThis chapter explains the basic principle of the instrumen

4 Description of function26 R-210/215 Operation Manual, Version Fc Cooling areaThe solvent vapor flows very quickly into the condenser. Here, the ener

4 Description of function27 R-210/215 Operation Manual, Version F4.1.3 Rear connections of the Rotavapor1234a Power supply for Rotavaporb Socket fo

4 Description of function28 R-210/215 Operation Manual, Version F4.3 Heating bathThe heating bath B-491 is multifunctional and can be used as a wate

4 Description of function29 R-210/215 Operation Manual, Version F4.5 Vapor temperature sensorFig. 4.7: Vapor temperature sensorThe vapor temperature

Table of contents3 R-210/215 Operation Manual, Version FTable of contents1 About this manual . . . . . . . . . . . . . . . . . . . . . . . . . . . .

4 Description of function30 R-210/215 Operation Manual, Version F4.7 Valve unitIf using the Rotavapor without the Vacuum Pumps V-700/710, or with a

4 Description of function31 R-210/215 Operation Manual, Version F4.10 Infrared interface12a Receiverb TransmitterFig. 4.12: Infrared interfaceThe in

5 Putting into operation32 R-210/215 Operation Manual, Version F5 Putting into operationThis chapter describes how the instrument is installed and g

5 Putting into operation33 R-210/215 Operation Manual, Version FSaving energyFor heating baths there are various ways to save energy. By using floatin

5 Putting into operation34 R-210/215 Operation Manual, Version F12345a Water inletb Water outletc Water level indicationd Level adjustment for the re

5 Putting into operation35 R-210/215 Operation Manual, Version F5.4 Glass assemblyTo install the glass assembly, consider the following:• To faste

5 Putting into operation36 R-210/215 Operation Manual, Version F5.6 Installing the reflux insert12345 Fig. 5.6: Installing the reflux insertTo install

5 Putting into operation37 R-210/215 Operation Manual, Version F5.8 Tube connections5.8.1 Connection scheme34264178958a Mains connectionb Communica

5 Putting into operation38 R-210/215 Operation Manual, Version F5.8.2 Cooling water tubesWhen connecting the white cooling water tubes, consider the

5 Putting into operation39 R-210/215 Operation Manual, Version F5.8.4 Tube connections to the valve unitTo connect the valve unit electrically, proc

Table of contents4 R-210/215 Operation Manual, Version F4 Description of function . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 Putting into operation40 R-210/215 Operation Manual, Version F5.9 Installing the vacuum controller321To install the vacuum controller on the Rotav

5 Putting into operation41 R-210/215 Operation Manual, Version F5.11 Installing the vapor temperature sensor1To measure the vapor temperature during

6 Operation42 R-210/215 Operation Manual, Version F6 OperationThis chapter explains the operating elements and possible operating modes. It gives ins

6 Operation43 R-210/215 Operation Manual, Version F6.1.3 Switching the B-491 from oil bath mode to water bath modeTo switch the heating bath from oil

6 Operation44 R-210/215 Operation Manual, Version F6.2 Immersion angle of the evaporating flask into the heating bath123The immersion angle into the h

6 Operation45 R-210/215 Operation Manual, Version F6.3 Lowering and raising the evaporating flask into and out of the heating bath123The stop-position

6 Operation46 R-210/215 Operation Manual, Version FΔ T2 (min. 20 °C)Δ T1 (min. 20 °C)Fig. 6.5: 20-40-60 ° rule6.5 DistillingTo start operating the in

6 Operation47 R-210/215 Operation Manual, Version FATTENTIONRisk of overflowing.• When you are operating with a 5 l heating bath, make sure that the

6 Operation48 R-210/215 Operation Manual, Version F6.7 When the distillation “dies out”When the distillation “dies out”, replace the receiving flask t

7 Maintenance and repairs49 R-210/215 Operation Manual, Version F7 MaintenanceThis chapter gives instructions on all maintenance work to be performe

Table of contents5 R-210/215 Operation Manual, Version F7 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 Maintenance and repairs50 R-210/215 Operation Manual, Version F7.3.1 Cleaning the sealsTo prolong the lifetime of the seals, rinse them regularly

8 Troubleshooting51 R-210/215 Operation Manual, Version F8 TroubleshootingThis chapter helps to resume operation after a minor problem has occurred w

8 Troubleshooting52 R-210/215 Operation Manual, Version FTable 8-1: General malfunction and their remedySealing system has been installed incorrectlyC

8 Troubleshooting53 R-210/215 Operation Manual, Version FTable 8-4: Error messages RotavaporError number Displayed at Possible cause RemedyE10 R-215 L

8 Troubleshooting54 R-210/215 Operation Manual, Version F8.2 Customer serviceOnly authorised service personnel are allowed to perform repair work on

9 Shutdown, storage, transport and disposal55 R-210/215 Operation Manual, Version F9 Shutdown, storage, transport and disposalThis chapter instructs

9 Shutdown, storage, transport and disposal56 R-210/215 Operation Manual, Version F9.3 Health and safety clearance formDeclaration concerning safety

10 Spare parts57 R-210/215 Operation Manual, Version F10 Spare partsThis chapter lists spare parts, accessories, and optional extras, including all

10 Spare parts58 R-210/215 Operation Manual, Version F10.1 Glass assembly AFig. 10.1: Glass assembly ATable 10-1: Glass assemblies AProduct Order nu

10 Spare parts59 R-210/215 Operation Manual, Version F10.2 Glass assembly VFig. 10.2: Glass assembly VTable 10-2: Glass assemblies VProduct Order nu

1 About this manual6 R-210/215 Operation Manual, Version F1 About this manualThis manual describes the Rotavapor and provides all information requir

10 Spare parts60 R-210/215 Operation Manual, Version F10.3 Glass assembly CFig. 10.3: Glass assembly C

10 Spare parts61 R-210/215 Operation Manual, Version FTable 10-3: Glass assemblies CProduct Order number Product Order numberGlass assembly C05 compl

10 Spare parts62 R-210/215 Operation Manual, Version F10.4 Glass assembly SFig. 10.4: Glass assembly S

10 Spare parts63 R-210/215 Operation Manual, Version FTable 10-4: Glass assemblies SProduct Order number Product Order numberGlass assembly S complet

10 Spare parts64 R-210/215 Operation Manual, Version F10.5 Glass assembly CRFig. 10.5: Glass assembly CR

10 Spare parts65 R-210/215 Operation Manual, Version FTable 10-5: Glass assemblies CRProduct Order number Product Order numberGlass assembly CR compl

10 Spare parts66 R-210/215 Operation Manual, Version F10.6 Glass assembly EFig. 10.6: Glass assembly E

10 Spare parts67 R-210/215 Operation Manual, Version FTable 10-6: Glass assemblies EProduct Order number Product Order numberGlass assembly E complet

10 Spare parts68 R-210/215 Operation Manual, Version F10.7 Glass assembly BYFig. 10.7: Glass assembly BY

10 Spare parts69 R-210/215 Operation Manual, Version FTable 10-7: Glass assemblies BYProduct Order number Product Order numberGlass assembly BY compl

2 Safety7 R-210/215 Operation Manual, Version F2 SafetyThis chapter points out the safety concept of the instrument and contains general rules of beh

10 Spare parts70 R-210/215 Operation Manual, Version F10.9 Various glass partsTable 10-9: Vacuum connectionProduct Order numberVacuum connection inc

10 Spare parts71 R-210/215 Operation Manual, Version FTable 10-13: Vapor ducts short for condenser V, C, S, E, CR, BYStandard joints without Combi C

10 Spare parts72 R-210/215 Operation Manual, Version FTable 10-17: Receiving flaskContent uncoated P+G P+G low temperature50 mL 00421100 mL 00422250 m

10 Spare parts73 R-210/215 Operation Manual, Version FTable 10-20: Distillation spider with 5 flasksContent Order number50 mL with SJ 24/29 01332100 m

10 Spare parts74 R-210/215 Operation Manual, Version FTable 10-25: CoverProduct Order numberTop cover B-491 48230Table 10-26: Water control valve ½”P

10 Spare parts75 R-210/215 Operation Manual, Version FTable 10-31: Control/communication cablesProduct Order numberControl cable between vacuum contr

11 Declarations and requirements76 R-210/215 Operation Manual, Version F11 Declarations and requirements11.1 FCC requirements (for USA and Canada)E

11 Declarations and requirements77 R-210/215 Operation Manual, Version F11.2 Declaration of conformity

2 Safety8 R-210/215 Operation Manual, Version F2.4 Warning notices used in this manualWARNINGGenerally, the triangular warning symbol indicates the p

2 Safety9 R-210/215 Operation Manual, Version FWARNINGPotential explosion risk if solvent vapors accumulate within the instrument housing.• Always us