Buchi Rotavapo R-100 Manual de usuario Pagina 4
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Contents BÜCHILabortechnikAG
iv OperationManualRotavapor®R100
5 Installation..........................................................................................................................21
5.1 Installationsite................................................................................................................................... 21
5.2 Mountingtherotarydriveunit ............................................................................................................ 21
5.3 Fittingthevaporductandcondenser ................................................................................................ 22
5.4 Fittingtheglassstopcock .................................................................................................................. 23
5.5 Connectingthevacuumandcoolingmediatubing............................................................................ 24
5.6 Electricalconnections........................................................................................................................ 25
5.7 Overviewofconnections.................................................................................................................... 25
5.8 Settingupandfillingtheheatingbath................................................................................................ 26
5.9 Quickcheck ....................................................................................................................................... 26
6 Operation............................................................................................................................27
6.1 Preparations ...................................................................................................................................... 27
6.1.1 Preparingtheheatingbath.....................................................................................................27
6.1.2 Fittingtheevaporatingflask................................................................................................... 28
6.1.3 Adjustingimmersionangleofevaporatingflask..................................................................... 29
6.1.4 Fittingthereceivingflask .......................................................................................................30
6.1.5 Verticaladjustment ................................................................................................................30
6.2 Performingdistillation ........................................................................................................................ 32
6.2.1 Raisingandloweringtheevaporatingflask ...........................................................................33
6.2.2 Adjustingdistillationconditions ..............................................................................................34
6.2.3 Optimizationdistillation ..........................................................................................................35
6.2.4 Feedingsolventduringdistillation..........................................................................................36
6.3 Finishingdistillation............................................................................................................................ 37
6.3.1 Removingtheevaporatingflask............................................................................................. 37
6.3.2 Removingthereceivingflask.................................................................................................38
7 Cleaningandservicing .....................................................................................................39
7.1 Inspectingandcleaningthevaporduct ............................................................................................. 39
7.2 Checkingthesystemforleaks........................................................................................................... 39
7.3 Checkingseals .................................................................................................................................. 40
7.4 Cleaningthecondenser..................................................................................................................... 40
7.5 Cleaningtheheatingbath.................................................................................................................. 41
7.6 Removingsolventaccumulations ...................................................................................................... 41
8 Helpwithfaults ..................................................................................................................42
8.1 Faults,possiblecausesandremedies............................................................................................... 42
8.2 Remedy ............................................................................................................................................. 44
8.2.1 Resettingoverheatsafetycutout .......................................................................................... 44
8.2.2 Replacingthefuse .................................................................................................................45
9 Takingoutofserviceanddisposal..................................................................................46
9.1 Takingoutofservice.......................................................................................................................... 46
9.2 Disposal............................................................................................................................................. 46
10 Appendix ............................................................................................................................47
10.1 Solventtable...................................................................................................................................... 47
10.2 Sparepartsandaccessories ............................................................................................................. 48
10.2.1 GlassapparatusV .................................................................................................................49
10.2.2 GlassapparatusC .................................................................................................................50
10.2.3 Accessories............................................................................................................................51
10.2.4 Wearparts .............................................................................................................................55
10.2.5 Spareparts ............................................................................................................................56
10.3 Listofabbreviations........................................................................................................................... 57
10.4 Healthandsafetyapproval................................................................................................................ 57
10.5 Healthandsafety............................................................................................................................... 58
- Rotavapor®R100 1
- OperationManual 1
- Contents 3
- 1 Aboutthisdocument 5
- 1.3 Availablelanguages 6
- 1.4 Trademarks 6
- 2 Safety 7
- 2.3 Staffqualification 8
- 2.4 Residualrisks 8
- 2.6 Modifications 10
- 3 Productdescription 11
- 3.2 Configuration 12
- Fig.3:Rearview R100 13
- Recirculating 14
- Chiller F-100 14
- 3.3 Specificationssupplied 16
- 3.4 Technicaldata 17
- 3.5 Safetyfeatures 19
- 4 Transportandstorage 20
- 5 Installation 21
- 5.6 Electricalconnections 25
- 5.7 Overviewofconnections 25
- IMPORTANT 26
- 6 Operation 27
- CAUTION 31
- WARNING 32
- 6.3 Finishingdistillation 37
- 7 Cleaningandservicing 39
- 7.3 Checkingseals 40
- 7.4 Cleaningthecondenser 40
- 8 Helpwithfaults 42
- 9.1 Takingoutofservice 46
- 9.2 Disposal 46
- 10 Appendix 47
- 10.3 Listofabbreviations 57
- 10.5 Healthandsafety 58
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