Buchi DuMaster D-480 Manual de usuario Pagina 1

Busca en linea o descarga Manual de usuario para Instrumentos de medición Buchi DuMaster D-480. BUCHI DuMaster D-480 User Manual Manual de usuario

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Indice de contenidos

Pagina 1 - Operation Manual

DuMaster D-480Operation Manual11593626 en

Pagina 2

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 10 Column properties (Dialog) ...

Pagina 3 - Copyright Note 3

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 100 Prioritizing urgent samples Via Edit > Swap you

Pagina 4

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 101 The following import options are available:  Imp

Pagina 5 - Contents

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 102 Performing other administrator tasks Target group

Pagina 6 - Contents 6

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 103 Modifying the registration Dialog: "Product r

Pagina 8 - Contents 8

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel authorized by BÜCHI Labortechnik AG and having undergone training. Purpose This

Pagina 9 - Contents 9

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 106 Setting up and starting up the instrument Target

Pagina 10 - Contents 10

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 107 Rules for first-time start-up First-time start-u

Pagina 11 - Contents 11

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 108  Room temperature should be constant.  Analy

Pagina 12

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 109 Category Type Part of initial equipment Carrier

Pagina 13 - General

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 11 Statistics > Clear statistic (Command) ...

Pagina 14 - Revision history

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 110  Filling the drying tube (on page 234).  Fil

Pagina 15 - About this document

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 111 Peripherals  A PC must be connected. It is ess

Pagina 16 - Display conventions

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 112 Detail of the rear The following picture shows a

Pagina 17 - Basic security settings

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 113 Removing the furnace transport protection Procee

Pagina 18

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 114  Push the left side door open from inside (mag

Pagina 19 - Warning: residual risks

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 115 CO2 intake pressure CO2 intake pressure is set a

Pagina 20 - Instrument casing

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 116 Shutting down the instrument Target group Person

Pagina 21 - Waste gas lines

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 117 Shutting the instrument down for short measuring

Pagina 22 - Meaning of the warning signs

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Heating up the furnace / checking parameters 118  In case the analyzer has to be transported, m

Pagina 23 - Knowledge and skills

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel with basic knowledge of chemistry and experience with laboratory work, e. g. ch

Pagina 25 - Changing mode

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 120 Measurement settings Target group Personnel with basic knowledge of chem

Pagina 26 - Filling reaction tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 121 Defining keywords for blank and conditioning samples Keywords Names of b

Pagina 27 - Filling the drying tube

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 122  Click Close to close the dialog. Required substances Different amino

Pagina 28

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 123 Specifying the computation method for blank value and daily factor Defin

Pagina 29 - Product description

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 124  ... switch off a signal, uncheck the appropriate checkbox.  Click O

Pagina 30 - 3 - Product description 30

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 125 Preparing samples Target group Personnel with basic knowledge of chemist

Pagina 31 - Technical specifications

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 126 Sample preparation instructions Samples with potential risks Various sam

Pagina 32 - Ambient conditions

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 127 The result will be that the nitrogen content is well measurable and you

Pagina 33 - Instrument design

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 128 Packing fatty, humid and non-pelletizeable solid samples - packing with

Pagina 34 - Front view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 129 Preparing measurement work Target group Personnel with basic knowledge o

Pagina 35 - Furnace section

Operation Manual D-480 ©BÜCH Labortechnik AG Purpose This chapter contains general topics of the document. In this chapter Revision history ...

Pagina 36 - Rear view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 130 Software usage rules Software usage rules Observe th following rules in

Pagina 37 - Right side view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 131  The carrier gas is reactivated and the furnaces are heated up to thei

Pagina 38 - Left side view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 132  Open the "Methods" dialog in the operating software by sele

Pagina 39 - Top view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 133 Copy methods Defining custom methods The existing method can be copied

Pagina 40

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 134  ... "Auto-decrement the number in the sample name": Works t

Pagina 41 - CHAPTER 4

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 135  This closes the dialog and the samples are swapped in the sample memo

Pagina 42

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 136 Performing measurement work Target group Personnel with basic knowledge

Pagina 43 - Functional units

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 137 Values for oxygen dosing Meaning of oxygen dosing The following illustra

Pagina 44 - dosing system (I)

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 138 Animal feed, approx. 500 mg medium fat content 50 mgFeed 250 ml/min, 1

Pagina 45

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 139 When is routine measuring work necessary? You must perform routine measu

Pagina 46

Operation Manual D-480 ©BÜCH Labortechnik AG 1 - General 14 Revision history List of modifications in this document up to now Date Modification

Pagina 47

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 140  Save the data or print them out. See Data backup and printing (on pag

Pagina 48 - Introduction

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 141 Definitions Routine measuring work comprises the following activities: 

Pagina 49

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 142  Measure a maximum of 50 real samples.  At the end of the series, me

Pagina 50 - Setting device parameters

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 143 Checklist Go through the following list:  Were the results of a blank

Pagina 51 - Instrument equipment

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 144  The N integral values should be between 10 and 50 after stabilization

Pagina 52

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 145  Name: Blnk  Weight: 1 mg  Click Method in the line of the appropr

Pagina 53

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 146  Allocate the daily factor to the real samples in the sample view (tex

Pagina 54

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 147  Click OK. "Standard tolerance monitoring" is now enabled.

Pagina 55 - Calibration formulae

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 148 Preparing measuring data for evaluation Target group Personnel with basi

Pagina 56 - Routine measuring work

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 149 Configuring the sample view Configuring the sample view Proceed as follo

Pagina 57 - Daily factor determinations

Operation Manual D-480 ©BÜCH Labortechnik AG 1 - General 15 About this document Status of the operating instructions The status of the operating i

Pagina 58 - Daily factor

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 150 Saving the sample view Saving the sample view Proceed as follows:  Ope

Pagina 59

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 151  You can generate statistical data manually. In this case, the user co

Pagina 60

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 152 Mean value The mean value of "n" element concentrations is com

Pagina 61 - Software user interface

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 153 Single peaks In general a single peak looks as follows: Superimposed pe

Pagina 62 - Sample view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 154 Manual integratability Regarding the integratability there are certain d

Pagina 63 - Color coding

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 155  Click and mark the peak end in the same way as described in the pre

Pagina 64 - Combi view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 156  The peak area was entered in the corresponding cell in the sample vie

Pagina 65

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 157 Setting the size of the graph with the mouse Proceed as follows:  Drag

Pagina 66 - Calibration view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 158 Data backup and printing Why backup and print data? The measuring data

Pagina 67 - Status view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 159 Overview of export and import file formats Export and import The analysi

Pagina 68

Operation Manual D-480 ©BÜCH Labortechnik AG 1 - General 16 Display conventions Before you start using this guide, it is important to understand t

Pagina 69 - Right mouse button function

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 160  Edit the imported data as required and save them when you are finishe

Pagina 70 - Further functions

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 161 Working with documents Target group Personnel with basic knowledge of ch

Pagina 71 - Copyright Note 71

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 162 Creating new documents Usual procedure Usually, one document is created

Pagina 72 - Copyright Note 72

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 163 Swap samples Proceed as follows:  Open the "Swap samples" di

Pagina 73 - 21 CFR Part 11 functionality

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 164  A message appears which informs that the coefficients included in the

Pagina 74 - Versioning

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 165 Importing documents Importing documents Proceed as follows:  Open the

Pagina 75 - Work performed by the system

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 166 Checking documents for authenticity What signature is checked? Only thos

Pagina 76 - Requirements for operation

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel authorized by BÜCHI Labortechnik AG and having undergone training. Purpose This

Pagina 77 - Configure analyzer

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 168 Important information about maintenance Target group Personnel au

Pagina 78 - Defining logon timeout

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 169 Maintenance work to be performed by the customer Note Observe tha

Pagina 79 - Creating new sections

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel working with the instrument. Purpose This section describes basic safety rules

Pagina 80

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 170 Viewing the status of maintenance intervals Viewing maintenance i

Pagina 81 - LIMS export settings

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 171 Status view message If the maximum number of measurements is reac

Pagina 82

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 172 Safety instruction Strictly observe the safety instruction &quo

Pagina 83 - Granting authorizations

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 173  Baking out tubes to remove moisture and contaminations from th

Pagina 84

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 174 Safety instruction Strictly observe the safety instruction &qu

Pagina 85 - Defining interfaces

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 175 Performing the calibration Target group Personnel authorized by B

Pagina 86

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 176 Viewing list of defined factor, monitor and standard samples View

Pagina 87 - Dialog details

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 177 Viewing calibration coefficients Viewing calibration coefficients

Pagina 88 - Editing analysis data

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 178 Process The section is divided into the following phases:  Prep

Pagina 89

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 179  Set oxygen dosing parameters (method) for conditioning and cal

Pagina 90 - Performing checks

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 18 Working with the operating instructions Operating the analyzer Read th

Pagina 91

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 180  Click OK to save your settings and close the dialog. The "

Pagina 92 - Viewing the logbook

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 181  If deleting has not had the desired effect, you can undo it. T

Pagina 93 - Working with the database

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 182 Assessing the calibration curves Calibration curve display in the

Pagina 94 - Database

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 183 The following table explains the characteristics relating to the

Pagina 95 - Database backup

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 184

Pagina 96 - Reorganize database

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 185 Calibration tables Target group Personnel authorized by BÜCHI Lab

Pagina 97

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 186 Calibration table for nitrogen calibration Suggestion The followi

Pagina 98

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 187 Replacing the ash crucible Target group Personnel authorized by B

Pagina 99 - Sleep/wake-up behavior

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 188 Purpose and frequency of crucible replacement Why replace the ash

Pagina 100

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 189 Furnace area The following picture shows the details of the furna

Pagina 101 - Optimizing data evaluation

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 19  Read the instructions on the individual chemicals in the safety dat

Pagina 102

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 190  Press the post combustion tube plug (1) and the combustion tub

Pagina 103 - Printer setup

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 191  Place the ash crucible in the tube rack into the vent or else

Pagina 104

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 192  Insert the new ash crucible into the combustion tube (4).  P

Pagina 105 - CHAPTER 6

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 193 Replacing sealing elements Target group Personnel authorized by B

Pagina 106

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 194 When to replace sealing elements What sealing elements are used?

Pagina 107 - General requirements

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 195 Visual o-ring/quad ring check You can tell when o-rings or quad r

Pagina 108 - Specific requirements

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 196 Ball valve maintenance Target group Personnel authorized by BÜCHI

Pagina 109 - Start-up

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 197 Removing and dismantling the ball valve Note The following sectio

Pagina 110 - Connecting peripherals

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 198 Furnace area The following picture shows the details of the furna

Pagina 111 - Configuring the balance

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 199 Furnace area The following picture shows the details of the furna

Pagina 112

ImprintProduct Identification: Operation Manual, DuMaster D-480 11593626 enBÜCHI Labortechnik AG Meierseggstrasse 40 Postfach CH-9230 Flawil 1E-Mail: q

Pagina 113

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 20  Contact with the substances may lead to chemical burns or poisoning

Pagina 114 - Default instrument settings

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 200 Phase 4: Dismantling the ball valve Please observe the following

Pagina 115 - Flow rate

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 201  Remove the ball and top half shell by means of the "knock

Pagina 116 - Shutting down the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 202 Process The section is divided into the following phases:  Clea

Pagina 117 - Procedure

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 203 Phase 2: Assembling the ball valve Proceed as follows:  Slighly

Pagina 118 - Safety instruction

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 204 Furnace area The following picture shows the details of the furna

Pagina 119 - Using the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 205 Maintaining the Ni flap and the O2 lance Target group Personnel a

Pagina 120 - Measurement settings

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 206 Purpose and frequency of maintaining the Ni flap and O2 lance Why

Pagina 121 - Viewing the list

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 207 Furnace area The following picture shows the details of the furna

Pagina 122

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 208 Phase 2: Removing the Ni flap (continued) Proceed as follows: 

Pagina 123

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 209 Installing the Ni flap Note The following section is a continuati

Pagina 124 - Configuring error handling

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 21  Front door  Left side door  Rear wall  Instrument cover. The

Pagina 125 - Preparing samples

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 210  Place the ungreased seal on the combustion tube connection (3)

Pagina 126 - Determining sample weight

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 211 Process This maintenance work is always carried out together with

Pagina 127 - Packing samples

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 212 Installing the O2 lance Proceed as follows:  Pull on the lance

Pagina 128

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 213 Removing, cleaning and installing the quartz glass bridge Target

Pagina 129 - Preparing measurement work

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 214 Removing the quartz glass bridge Process The section is divided i

Pagina 130 - Waking up the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 215 When to clean the quartz glass bridge The quartz glass bridge mus

Pagina 131 - Defining custom methods

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 216 Note: When you close a ground-in ball-and-socket joint, you must

Pagina 132 - Defining the Kjeldahl factor

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 217 Removing, cleaning and installing the carousel Target group Perso

Pagina 133 - Settings for sample input

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 218 Removing, cleaning and installing the carousel Purpose of cleanin

Pagina 134 - Prioritizing urgent samples

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 219  Lift off the ring at the pilots.  Clean the plastic top se

Pagina 135 - What can you optimize?

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 22 Warning signs on the analyzer Warning sign furnace The following pictu

Pagina 136 - Performing measurement work

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 220 Emptying and filling reaction tubes Target group Personnel author

Pagina 137 - Values for oxygen dosing

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 221 Emptying reaction tubes Requirements: Before starting work, the f

Pagina 138 - Performing measurements

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 222 Filling the combustion tube Note Note the following rules:  O

Pagina 139

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 223  Pour the recommended amounts of copper oxide (CuO) and corundu

Pagina 140 - Overview

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 224  Insert the wire mesh ronde.  Fill the chemicals through the

Pagina 141

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 225 Filling the reduction tube Proceed as follows:  Furnish both pl

Pagina 142 - Checklist

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 226 Removing/installing and conditioning the reaction tubes In this s

Pagina 143 - Background

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 227 Removing the reaction tubes from the furnace Process The section

Pagina 144 - Determining blank values

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 228 Top view furnace The following picture shows a top view of the fu

Pagina 145 - Determining the daily factor

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 229  Remove the quartz glass bridge. Hold the quartz glass bridge a

Pagina 146

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 23 Warning: changes to the instrument Safe instrument The analyzer is des

Pagina 147 - Stopping continuous analysis

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 230 Top view furnace The following picture shows a top view of the fu

Pagina 148

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 231 Note: When you close the ground-in ball-and-socket joints, you mu

Pagina 149 - Configuring the sample view

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 232  Close the front door. Phase 2: Conditioning the reaction tube,

Pagina 150 - Generating statistical data

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 233 Filling, removing and installing the absorption and drying tubes

Pagina 151 - Statistical data

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 234 Filling the drying tubes Note Note the following rules:  Observ

Pagina 152 - Manual peak integration

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 235 Drying tube filling (large) The following picture shows the filli

Pagina 153 - Melted peaks

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 236 Notes regarding further operation The drying tube fillings must b

Pagina 154 - Integration of single peaks

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 237 To prepare the instrument for maintenance work follow the instruc

Pagina 156 - Configuring the graph view

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel authorized by BÜCHI Labortechnik AG and having undergone training. Purpose This

Pagina 157 - Display print preview

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 24 Required personal safety equipment Protective glasses You require prot

Pagina 158 - Data backup and printing

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 240 Interpreting PC error messages Software reaction to errors When an e

Pagina 159 - Export and import

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 241 Interpreting combustion module error messages and troubleshooting Th

Pagina 160 - Exporting LIMS data

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 242 Performing a leak test Purpose of the leak test The leak test checks

Pagina 161 - Working with documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 243 Leak test procedure Process The execution of the leak test takes pla

Pagina 162 - Editing documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 244 F7 + F8 Furnace transformer 15 A Process The section is divided in

Pagina 163 - Finding documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 245 Phase 2: Remove and check fuse Proceed as follows:  If a part of t

Pagina 164 - Inserting data

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 246  The electrical section is now visible.  Pull out the fuse hol

Pagina 165 - Signing documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 247  Plug the protective earth conductor back into the rear wall. 

Pagina 166 - Checking a signature

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 248 Reacting to a power failure Open document An open document is not lo

Pagina 167 - Maintaining the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 249  Perform a leak test by selecting Options > Diagnostics > Le

Pagina 168

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 25 Damaged base panel Please observe the following instruction: Caution

Pagina 169 - Recommendation

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 250 Checking air-tightness of instrument Proceed as follows:  Perform

Pagina 170

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 251  Weigh the sample If the weight is not transmitted online, enter t

Pagina 171 - Installing used tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 252 Exporting analysis data Proceed as follows:  Open the "Export

Pagina 172 - Types of conditioning

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel involved with the instrument. Purpose This section describes the dialogs and co

Pagina 173 - Flushing tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 254 Dialog descriptions key Element types The following list provid

Pagina 174

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 255 File menu Purpose This section describes commands and dialogs f

Pagina 175 - Performing the calibration

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 256 File > New (Command) What is the command used for? This comm

Pagina 176 - Defining standard substances

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 257 Label Element type Meaning Mode Dropdown listbox Field in whi

Pagina 177

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 258 Label Element type Meaning Signatures Listbox column Column d

Pagina 178 - Requirements:

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 259 Further information Further information includes instructions i

Pagina 179

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 26 Removing reaction tubes Please observe the following instructions: War

Pagina 180

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 260 File > Delete (Command) What is the command used for? This c

Pagina 181

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 261 Sign (Dialog) Function In the dialog:  the user is warned abo

Pagina 182 - Displayed characteristics

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 262 Open You can open this dialog, if 21 CFR Part 11 functionality

Pagina 183 - Coefficient "a"

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 263 Label Element type Meaning Cancel Button Aborts the process an

Pagina 184

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 264 Open Open the dialog via: Menu command Button Hot key File >

Pagina 185 - Calibration tables

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 265 Print (Dialog) Function In this dialog you can define print s

Pagina 186 - Suggestion

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 266 Remaining elements: Label Element type Meaning OK Button Start

Pagina 187 - Replacing the ash crucible

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 267 Printer setup (Dialog) Function In this dialog you can specify

Pagina 188 - Removing the ash crucible

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 268 Open (Dialog) Function In this dialog you can specify the follo

Pagina 189 - Top view furnace

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 269 Load balance file (Dialog) Function In this dialog you can sele

Pagina 190

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 27 Warning Harmful substances when glass is broken! When filled quartz o

Pagina 191 - Installing the ash crucible

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 270 In section "Backup": Label Element type Meaning Selec

Pagina 192

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 271 Clean database (Dialog) Function In the dialog:  the user is

Pagina 193 - Replacing sealing elements

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 272 Caution Data loss! Restoring the database via Restore irrevoca

Pagina 194

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 273 Label Element type Meaning Cancel Button Aborts the process or

Pagina 195 - Removing sealing elements

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 274 Edit menu Purpose This section describes commands and dialogs f

Pagina 196 - Ball valve maintenance

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 275 Edit > Redo (Command) What is the command used for? This com

Pagina 197

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 276 Short cuts Invocation via the toolbar: Invocation via hot key

Pagina 198

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 277 Short cuts Invocation via the toolbar: Note The line to delet

Pagina 199 - Dismantled ball valve

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 278 If 21 CFR Part 11 functionality is enabled, a new version of th

Pagina 200

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 279  by clicking the right mouse key to the corresponding sample

Pagina 201

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 28 Overheating of tube fillings Please observe the following instruction:

Pagina 202 - Requirements

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 280 Note After invoking this command the dialog "Recalculate H

Pagina 203

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 281 View menu Purpose This section describes commands and dialogs f

Pagina 204

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 282 View > Toggle (Command) What is the command used for? This c

Pagina 205

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 283 Elements The following describes the elements of the dialog. La

Pagina 206

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 284 Elements The following describes the elements of the dialog. La

Pagina 207

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 285 Load views (Dialog) Function In this dialog you can reload save

Pagina 208

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 286 View > Gridview > Auto align (Command) What is the comman

Pagina 209 - Installing the Ni flap

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 287 Further information Further information includes instructions i

Pagina 210

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 288 Further information Further information includes instructions i

Pagina 211

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 289 System menu Purpose This section describes commands and dialogs

Pagina 212 - Installing the O

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel working with the instrument. Purpose This section provides general information

Pagina 213

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 290 System > Auto run (Command) What is the command used for? Th

Pagina 214

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 291 Note The "Abort analysis" dialog appears. Observe the

Pagina 215

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 292 Label Element type Meaning Cancel Button Aborts the process. F

Pagina 216

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 293 Label Element type Meaning Position Radiobutton Moves the car

Pagina 217

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 294 Further information Further information includes instructions i

Pagina 218 - Cleaning the carousel

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 295 Windows menu Purpose This section describes commands and dialog

Pagina 219

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 296 Windows > Toolbar / Run-Bar (Command) What are these command

Pagina 220

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 297 Icon Command Calibration > Next sample System > Wake-up

Pagina 221 - Emptying reaction tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 298 Label Element type Meaning No. Label Displays the number of t

Pagina 222 - Filling the combustion tube

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 299 Options menu Purpose This section describes commands and dialog

Pagina 223

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 3 Copyright © BÜCHI Labortechnik AG All rights reserved This document contains propri

Pagina 224 - Filling the reduction tube

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 30 Analytical characteristics and technical specifications Target group Perso

Pagina 225

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 300 Maintenance intervals (Dialog) Function In this dialog, any num

Pagina 226 - In this section

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 301 Further information Further information includes instructions i

Pagina 227

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 302 Commands for the maintenance of the liquid sampler VLS Commands

Pagina 228

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 303  Maintenance work to be performed by the customer (on page 16

Pagina 229

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 304 In the lower area: Label Element type Meaning Result Label Th

Pagina 230

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 305 Label Element type Meaning Apply Button Heats up the correspon

Pagina 231

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 306 Remaining elements: Label Element type Meaning Close Button Cl

Pagina 232

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 307 Open Open the dialog via:  Options > Diagnostics > Erro

Pagina 233

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 308 Label Element type Meaning autom. Auto-increment the number in

Pagina 234 - Filling the drying tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 309 Label Element type Meaning Name Textbox/label Field to input

Pagina 235 - Drying tube filling (large)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 31 Analytical characteristics Analytical characteristics The following table

Pagina 236

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 310 Further information Further information includes instructions i

Pagina 237

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 311 Open Open the dialog via Options > Settings > Calculation

Pagina 238

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 312  If you are using multiple analyzers with one PC, you must sp

Pagina 239 - Repairing the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 313 In section "Network": Label Element type Meaning Path

Pagina 240 - Interpreting error code

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 314 Valid for all tabs: Remaining elements: Label Element type Mean

Pagina 241 - Performing a system test

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 315 Label Element type Meaning Peak anticipation Textbox Field to

Pagina 242 - Performing a leak test

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 316 Label Element type Meaning O2 dosing time Textbox Field to in

Pagina 243 - Replacing fuses

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 317 Elements The following describes the elements of the dialog. La

Pagina 244 - Fuse holder

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 318 In section "Sleep": Label Element type Meaning Sleep

Pagina 245

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 319 Monthly logbook (Dialog) Function This dialog contains records

Pagina 246 - Phase 3: Insert fuses

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 32 Interfaces USB, RS232 /V24, Safety low voltage as per DIN IEC 380/VDE 080

Pagina 247 - After a computer crash

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 320 Further information Further information includes instructions i

Pagina 248 - Reacting to a power failure

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 321 Safety instruction Strictly observe the safety instruction &q

Pagina 249

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 322 Entry Standard Description Parity N Defines the type of parity

Pagina 250

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 323 The following table describes the entries under the "Syste

Pagina 251 - Export for support

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 324 Label Element type Meaning OK Button Saves new settings Cancel

Pagina 252 - Exporting analysis data

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 325 Math menu Purpose This section describes commands and dialogs f

Pagina 253 - Menu and dialog descriptions

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 326 Math > Blank values > Calculate (Command) What is the com

Pagina 254 - Dialog descriptions key

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 327  Routine measuring work (on page 56)  Types of blank value

Pagina 255 - File menu

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 328 The dialog The appearance of the dialog depends on the selected

Pagina 256 - File > New (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 329 Elements The following describes the elements of the dialog. La

Pagina 257 - Listbox columns

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 33 Instrument design Target group Personnel involved with the instrument. Pur

Pagina 258 - Select version (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 330 Math. > Recalculate (Command) What is the command used for?

Pagina 259 - Save file as (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 331 Statistics menu Purpose This section describes commands and dia

Pagina 260 - File > Delete (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 332 Statistics > Via names (Command) What is the command used fo

Pagina 261 - Sign (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 333 Statistics > Include/Exclude sample (Command) What is the co

Pagina 262 - Export to LIMS (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 334 Calibration menu Purpose This section describes commands and di

Pagina 263 - Configure report (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 335 Calibration coefficients (Dialog) Function This dialog displays

Pagina 264 - Further information

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 336 Label Element type Meaning Cancel Button Discards calibration

Pagina 265 - Print (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 337 Further information Further information includes instructions i

Pagina 266 - Print preview (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 338 Calibration > Next sample (Command) What is the command us

Pagina 267 - Printer setup (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 339 Help menu Purpose This section describes commands and dialogs f

Pagina 268 - Open (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 34 Front view Front view, closed The following picture shows the front view o

Pagina 269 - Configure backup (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 340 Help > Content (Command) What is the command used for? This

Pagina 270

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 341 In section "Analyzer": Label Element type Meaning Typ

Pagina 272 - Log in as (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel involved with the instrument. In this chapter Warranty ...

Pagina 273 - File > Exit (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 344 Warranty Target group Personnel involved with the instrument. In this section Warr

Pagina 274 - Edit menu

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 345 Warranty of the overall instrument Warranty of the overall instrument Please refer

Pagina 275 - Edit > Copy (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 346 Accessories, spare parts and consumables Target group Personnel involved with the i

Pagina 276 - Edit > Paste (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 347 Smallest workable unit Condition You can only order the smallest workable unit if y

Pagina 277 - Edit > Modify (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 348 Computer A computer is essential as the control and evaluation unit. The computer c

Pagina 278 - Set stop tag (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 349 Consumables set for solid samples  Optional  Required when the material from th

Pagina 279

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 35 Furnace section Location of the furnace section The furnace section is loc

Pagina 281 - View menu

Operation Manual D-480 ©BÜCH Labortechnik AG Index 351 2 21 CFR Part 11 functionality - 73, 94, 259, 260, 261, 262, 320 A About this document - 15

Pagina 282 - Configure view (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Index 352 Defining the balance / PC interface - 87 Defining the Kjeldahl factor - 132 Defining the LI

Pagina 283 - Column properties (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Index 353 Loading a sample view - 150, 285 Log in as (Dialog) - 272 M Maintaining the instrument - 16

Pagina 284 - Save views (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Index 354 Selecting the operating mode - 110, 131, 294 Set current weighed sample (Dialog) - 279 Set

Pagina 286 - Function

Technical data are subject to change without notice/Quality Systems ISO 9001.The English version is the original language version and serves as basis

Pagina 287

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 36 Top view furnace The following picture shows a top view of the furnace pul

Pagina 288 - Select columns (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 37 Right side view Right side view, closed The following picture shows the ri

Pagina 289 - System menu

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 38 Left side view Left side view, closed The following picture shows the left

Pagina 290 - System > Stop (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 39 Top view Top view of the instrument The following picture shows the top vi

Pagina 293 - Analysis mode (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel with basic chemical knowledge and basic computer knowledge. Purpose This sectio

Pagina 294

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 42 Layout and mode of functioning Target group

Pagina 295 - Windows menu

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 43 Functional units Introduction The following

Pagina 296 - Toolbar

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 44 I Mechanical sample insertion and O2 dosing

Pagina 297 - Weighing window (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 45 6 Post combustion tube with tube filling 

Pagina 298

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 46 Processes in the instrument during a measure

Pagina 299 - Options menu

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 47 Sample insertion and initiation of measureme

Pagina 300

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 48  Volatile halogen compounds are bound on s

Pagina 301 - Replace part (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 49 Basic facts about working with the instrumen

Pagina 302 - Leak test (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 5 Contents CHAPTER 1 General 13 Revision history ...

Pagina 303

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 50 Setting device parameters About instrument p

Pagina 304 - System test (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 51 Instrument equipment Combustion tube filling

Pagina 305

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 52 Filling the post combustion tube The followi

Pagina 306 - Error display (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 53  The daily factor for a measuring componen

Pagina 307 - Input options (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 54 Linear calculation over the whole range The

Pagina 308 - Standard samples (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 55 Polynomial calculation over the whole range

Pagina 309 - Keywords (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 56 Computing calibration coefficients Once the

Pagina 310 - Acoustic signals (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 57 Routine measuring work is performed at set i

Pagina 311 - LIMS settings (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 58 Blank value determination In blank value det

Pagina 312 - "LIMS data" tab

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 59 Understanding the operating software Target

Pagina 313 - "Identifier" tab:

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 6 Understanding the operating software ...

Pagina 314 - Device parameters (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 60 Basic functions of the operating software In

Pagina 315 - Method (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 61 Software user interface The main window of t

Pagina 316 - Error handling (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 62  ... display the online help. Details on t

Pagina 317

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 63 View The sample view looks like a familiar c

Pagina 318

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 64 Sample not yet analyzed, but a sample name

Pagina 319 - Monthly logbook (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 65 Progression view (graph view) Progression v

Pagina 320 - Select period (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 66 Statistics view The statistics view display

Pagina 321 - "DEVICE.INI" tab

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 67 If your series includes samples previously d

Pagina 322

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 68 The areas of the status view and what they m

Pagina 323 - Configure key value (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 69 Copyright © BÜCHI Labortechnik AG All rights reserved This document contains propri

Pagina 324

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 7 Start-up ...

Pagina 325 - Math menu

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 70 In dialogs In dialogs you can also press the right mouse button to display certain

Pagina 326 - Blank values (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 71 Data administration and data security Target group Personnel with basic chemical kn

Pagina 327 - Define type of peak (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 72 Laboratory information and management system (LIMS) What does LIMS do? The Laborato

Pagina 328 - Area assignment (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 73 21 CFR Part 11 functionality What is 21 CFR Part 11? 21 CFR Part 11 is a regulation

Pagina 329

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 74 Restricted access to menu functions The software restricts access to the menu funct

Pagina 330

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel with good knowledge of the operating system and administrative settings. Purpos

Pagina 331 - Statistics menu

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 76 Installing and updating the software Conditions for

Pagina 332

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 77 Configure analyzer Target group Personnel with basi

Pagina 333

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 78 What can you modify in the configuration? Safety

Pagina 334 - Calibration menu

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 79 Creating new sections Safety instruction Strictly

Pagina 335

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 8 Setting the size of the graph ...

Pagina 336

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 80 Defining LIMS export settings Target group Personne

Pagina 337

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 81 LIMS export settings What is set? The following are

Pagina 338

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 82 Setting up user administration Target group Personn

Pagina 339 - Help menu

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 83 User administration User groups Access to menu func

Pagina 340 - Help > Find (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 84 Safety instruction Strictly observe the safety in

Pagina 341 - Short cuts

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 85 Defining interfaces Target group Personnel with goo

Pagina 342

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 86 Defining the analyzer / PC interface Note The opera

Pagina 343 - Appendix

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 87 Defining the balance / PC interface Safety instru

Pagina 344 - Warranty

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 88 Editing analysis data Target group Personnel with g

Pagina 345 - Warranty on the furnace

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 89 When does it make sense to edit analysis data? Reas

Pagina 346 - 11 - Appendix 346

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 9 Filling, removing and installing the absorption and drying tubes ...

Pagina 347 - Required accessories

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 90 Performing checks Target group Personnel with good

Pagina 348 - Optional accessories

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 91 Checking documents for authenticity What signature

Pagina 349 - 11 - Appendix 349

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 92 Viewing the logbook Viewing the logbook Proceed a

Pagina 350

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 93 Working with the database Target group Personnel wi

Pagina 351 - Index 351

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 94 Database What is a database? A database is characte

Pagina 352 - Index 352

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 95 Defining the autoexport directory Safety instruct

Pagina 353 - Index 353

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 96 Autoexport Autoexport creates a backup of the curre

Pagina 354 - Index 354

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 97 Reorganize database Proceed as follows:  Open the

Pagina 355

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 98 Ways of optimizing the use of the analyzer Target g

Pagina 356 - Find your BUCHI Contacts:

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 99 Optimizing basic instrument settings Analyzer confi

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